000			02062nam a2200217 4500
001			378129
090			_a378129
100			_a20210621u y0pory50 ba
101			_aeng
200			_aIdentification and determination of opioid peptides in biological material using the LC-QTOF-MS/MS technique _bRecurso eletrónico _fMagdalena PoPławska ...[et al.]
311			_aFicheiro de 520 KB em formato PDF.
330			_a1. Introduction. 2. Case report. 3. Materials and methods. 3.1. Reagents and reference materials. 3.2. Analytical material. 3.3. Equipment and analytical parameters. 3.4. Qualitative analyses. 3.5. Quantitative analysis of deltorphin I and II in the secretion of Phyllomedusa bicolor. 3.6. Quantitative analysis of deltorphin I and II in blood. 3.7. Isolation of deltorphins from blood. 3.8. Preparation of samples for analysis. 3.9. Solutions for the validation of a method for the determination of deltorphin I and II. 3.10. Validation of the method for the determination of deltorphin I and II in “kambo”. 3.11. Validation of the method for determination of deltorphins in blood. 3.12. Estimating the degradation of deltorphins in blood. 4. results. 4.1. Identification of deltorphin I and II in the analysed sample of secretion from the frog Phyllomedusa bicolor. 4.2. Results obtained for evaluated validation parameters. 4.3. Determination of deltorphin I and deltorphin II concentrations in frog secretion. 4.4. Estimating the degradation of deltorphins in blood. 4.5. Determination of deltorphin I and deltorphin II concentration in the blood sample. 5. Conclusions.
461			_d2018 _vVol. 116 _tProblems of Forensic Sciences _x1230-7483 _pp. 357–374
606			_aTOXICOLOGIA _9263124
606			_aANÁLISE LABORATORIAL _9326721
606			_aESPECTROMETRIA _9321956
710			_aIDENTIFICATION AND DETERMINATION OF OPIOID PEPTIDES IN BIOLOGICAL MATERIAL USING THE LC-QTOF-MS/MS TECHNIQUE _9351788