Identification and determination of opioid peptides in biological material using the LC-QTOF-MS/MS technique [Recurso eletrónico] / Magdalena PoPławska ...[et al.]
Autor institucional: IDENTIFICATION AND DETERMINATION OF OPIOID PEPTIDES IN BIOLOGICAL MATERIAL USING THE LC-QTOF-MS/MS TECHNIQUEIn: Problems of Forensic Sciences.ISSN 1230-7483. Vol. 116 (2018) , p. 357–374Idioma: Inglês.Assunto: TOXICOLOGIA | ANÁLISE LABORATORIAL | ESPECTROMETRIA Resumo: 1. Introduction. 2. Case report. 3. Materials and methods. 3.1. Reagents and reference materials. 3.2. Analytical material. 3.3. Equipment and analytical parameters. 3.4. Qualitative analyses. 3.5. Quantitative analysis of deltorphin I and II in the secretion of Phyllomedusa bicolor. 3.6. Quantitative analysis of deltorphin I and II in blood. 3.7. Isolation of deltorphins from blood. 3.8. Preparation of samples for analysis. 3.9. Solutions for the validation of a method for the determination of deltorphin I and II. 3.10. Validation of the method for the determination of deltorphin I and II in “kambo”. 3.11. Validation of the method for determination of deltorphins in blood. 3.12. Estimating the degradation of deltorphins in blood. 4. results. 4.1. Identification of deltorphin I and II in the analysed sample of secretion from the frog Phyllomedusa bicolor. 4.2. Results obtained for evaluated validation parameters. 4.3. Determination of deltorphin I and deltorphin II concentrations in frog secretion. 4.4. Estimating the degradation of deltorphins in blood. 4.5. Determination of deltorphin I and deltorphin II concentration in the blood sample. 5. Conclusions.| Item type | Current location | Call number | Status | Date due | Barcode |
|---|---|---|---|---|---|
| Analíticos de Periódicos | Biblioteca da Polícia Judiciária | PJCD 309 (Browse shelf) | Available |
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1. Introduction. 2. Case report. 3. Materials and methods. 3.1. Reagents and reference materials. 3.2. Analytical material. 3.3. Equipment and analytical parameters. 3.4. Qualitative analyses. 3.5. Quantitative analysis of deltorphin I and II in the secretion of Phyllomedusa bicolor. 3.6. Quantitative analysis of deltorphin I and II in blood. 3.7. Isolation of deltorphins from blood. 3.8. Preparation of samples for analysis. 3.9. Solutions for the validation of a method for the determination of deltorphin I and II. 3.10. Validation of the method for the determination of deltorphin I and II in “kambo”. 3.11. Validation of the method for determination of deltorphins in blood. 3.12. Estimating the degradation of deltorphins in blood. 4. results. 4.1. Identification of deltorphin I and II in the analysed sample of secretion from the frog Phyllomedusa bicolor. 4.2. Results obtained for evaluated validation parameters. 4.3. Determination of deltorphin I and deltorphin II concentrations in frog secretion. 4.4. Estimating the degradation of deltorphins in blood. 4.5. Determination of deltorphin I and deltorphin II concentration in the blood sample. 5. Conclusions.
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